48:49Refluxing a Reaction | MIT Digital Lab Techniques Manual
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Refluxing a Reaction Most organic reactions occur slowly at room temperature and require heat to allow them to go to completion in a reasonable time frame. Running a reaction under reflux allows you to heat a reaction without losing solvent due to evaporation and with causing an explosion. Created by Dr. Kimberly Berkowski and Eileen Huang. View the complete resource at:https://ocw.mit.edu/courses/res-5-0001-digital-lab-techniques-manual-spring-2007/ License: Creative Commons BY-NC-SA More information at http://ocw.mit.edu/terms More courses at http://ocw.mit.edu WARNING NOTICE: The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such safety procedures and measures. MIT shall have no responsibility, liability, or risk for the content or implementation of any of the material presented. Legal Notice - http://ocw.mit.edu/OcwWeb/web/terms/terms/index.htm
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